direction Vienna, Austria     email ralacaboard@red-ralaca.net

 

National Agricultural Laboratory in São Paulo (LANAGRO-SP)


 Contact person in the laboratory

 Maria de Fátima Martins Pinhel

 Email of contact person

 This email address is being protected from spambots. You need JavaScript enabled to view it.

 Mandate of the Laboratory:

 LANAGRO-SP is an Official Laboratory of MAPA - Ministry of   Agriculture, Livestock and Food Supply. It is to support, through   laboratory analysis, the inspection actions and monitoring programs   of the SDA - Agriculture and Livestock Defense Secretariat.

 Role in the farm-to-fork chain:

 The main role is to support MAPA’s policies such as to coordinate   and monitor technical studies, science and technology, analytical   tests and actions by trace, control, monitoring and evaluation   processes relating to the safety and quality of animal and vegetal   origin products, and animal health.

 National Reference Laboratory:

   Yes. LANAGRO-SP is an OIE reference laboratory for avian     influenza  and Newcastle disease diagnosis. As a national l   laboratory,  LANAGRO-SP also acts according to the MAPA’s policies   in official inspection programs, analysing products of animal origin,   animal feed, beverages, fertilizers, avian vaccines, anti- rabies   vaccines, veterinary drugs, pesticides and samples for avian   diagnosis, in order to ensure the safety and quality of the product for   domestic market, exporting and importing operations. Besides that,   LANAGRO- SP is reference laboratory to the PNCRC – National   Program for Residues and Contaminants Control, processing   samples of meat (poultry, cattle, swine, equine, and fish) and milk,   for exportation, importation and national trade. Other activities   includes the participation on audits in private laboratories of the   MAPA’s Network laboratories and research, development and   validation of laboratory methods.

 Type of contaminants analysed:

 ANIMAL AREA
 Residues of Veterinary Drugs
 Residues of Inorganic Contaminants
 Residues of Pesticides: Organochlorines pesticides and PCBs
 Microbial contaminants
 PLANT AREA
 Microbial contaminants

 Matrices analysed:

 Matrices of animal origin: meat of bovine, equine, swine, fish and   shrimp, poultry, ostrich, sheep, goat, rabbit; honey and milk.
 Matrices of plant area: beverages

 Combination matrices and contaminants
 analysed:

See attached table – Contaminants and Matrices/Species -
LANAGRO-SP 

 Description of validated method used:

Inorganic Contaminants Residues
- Determination of cadmium and lead (Cd and Pb) in meat by graphite furnace atomic absorption spectrometry (GF AAS)
-Determination of the inorganic contaminant arsenic (As) in meat by atomic absorption spectrometry with generation of hydrides (HG AAS)
- Determination of mercury in fish and meat by TDA AAS
- Determination of inorganic contaminants in fresh milk by ICP-MS

Organochlorine pesticide residues
- Determination of organochlorines pesticides and PCBs in animal fat by CG – ECD and CG-MS
- Determination of organochlorines pesticides and PCBs in fish muscle by CG – ECD and CG-MS

Veterinary drugs residues
- Determination of chloramphenicol in honey by LC-MS / MS
- Determination of thyrostatics in swine urine by LC-MS / MS
- Determination of ractopamine in swine urine by LC-MS / MS
- Determination of nitrofurans metabolites in poultry muscle by LC-MS / MS
- Determination of nitrofurans metabolites in equine muscle by LC-MS / MS
- Determination of nitrofurans metabolites in shrimp muscle by LC-MS / MS
- Determination of β-agonists in bovine urine by LC-MS / MS
- Determination of β-agonists in bovine and porcine muscle by LC-MS / MS

Microbial contaminants
-Presumptive detection of Salmonella spp. by polymerase chain reaction (AFNOR Validation nº BIO 18/03-11/02)
- Detection of Salmonella spp. (ISO 6579-1:2017)
- Coliform Count (ISO 4832:2006)
- Thermotolerant coliforms Count
- Most Likely Number of Coliforms (ISO 4831:2006)
- Detection, isolation and identification of Escherichia coli O157:H7 (MLG 5.09 e MLG 5A.04)
- Presumptive detection of Listeria monocytogenes by polymerase chain reaction (AFNOR Validation QUA 18/05-07/08)
- Presumptive count of Bacillus cereus (ISO 7932:2004)
- Count of Clostridium perfringens (ISO 7937:2004)
- Count of Staphylococcus aureus (BAM:2016)
- Detection and isolation of Escherichia coli producing Shiga toxin (STEC) non O157
(MLG 5B.05)
- Yeast and mold counts in products with water activity greater than 0,95 (ISO 21527-1:2008)
- Yeast and mold content in products with water activity less than or equal to 0,95 (ISO 21527-2:2008)

 Laboratory accredited according to
 ISO17025:

Yes 

 Provision of interpretation of residue
 data to customers:

 Yes

 Laboratory certified according to GLP:

 No



Laboratório de Análise e Detecção de Alimentos Irradiados (LADAI)



 Contact person in the laboratory:


 Anna Lucia Casañas Haasis Villavicencio


 Email:

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 Mandate of the Laboratory:

 Analysis on food irradiation: Physical, chemical, physico'chemical,   biochemical, biological, microbiological, toxicological, nutritional,   sensorial analysis, food irradiation detection and formation of new   compound in processed foods by radiation.


 Role in the farm-to-fork chain:

 We are involved in the farm-to-fork chain from the beginning using   nuclear technology in the phytosanitary field prevention as well as in   the industrial processing of food packaged "fresh" ready to eat, when   indicate that technology in order to provide safe food to consumers.


 National Reference Laboratory:

 Not yet.
 We are starting to improve new equipments to run in order
 to get accreditation with ISO 17025 


 Type of contaminants analysed:

 Insect and microbiological contamination, mycotoxin, volatile   compounds, hydrocarbons and alkyl cyclobutanones.

 Matrices analysed:

 Packaged Food in general as well as grains, tea, spices, fresh and   dehydrated fruits and vegetables, all kind of meat that countains   small amount of fat.
 

Combination matrices and contaminantsanalysed:

 Fat meat: alkyl cyclobutanones
 Fat fruits: alkyl cyclobutanones

Description of validated method used:

 EN 1784 (CG/MS)
 EN 1785 (2-ACB)
 EN 1786 (RPE bones)
 EN 1787 (RPE cellulose)
 EN 1788 (TL)
 EN 13708 (RPE aҫucar)
 EN 13783 (DEFT-APC)
 EN 13784 (comet)
 EN 14569 (LAL-GNB)

 Laboratory accredited according to
 ISO17025:

 Not yet 

 Provision of interpretation of residue
 data to customers:

 No 

Provision of interpretation of residue
data to customers:

 No

Laboratory certified according to GLP:

 Not yet

Is laboratory available for research and
development (R@D) within RALACA when funding becomes available?

 We hope yes

 

Is the laboratory available for quality auditing services within RALACA when funding becomes available?


 We expect yes


 

Is the laboratory available for expert missions within RALACA when funding becomes available?

 
 Yes

 

Is the laboratory available for ad hoc on-site training when funding becomes available?

 Yes

Is the laboratory available for ad hoc
remote/distance learning training when technology and funding becomes
available?


 Yes

Is the laboratory available for preparation of ad hoc reference materials when projects/funding becomes available?


 Yes

Is the laboratory available for organization and distribution of ad hoc proficiency testing/collaborative trials when projects/funding becomes available?

 Yes

 
Center of Research and Analysis of Residue and Contaminants (CEPARC)

 Contact person in the laboratory

 Ionara Regina Pizzutti

 Email of contact person

 This email address is being protected from spambots. You need JavaScript enabled to view it.

 Type of contaminants analysed:

 Mainly Pesticides and Mycotoxins

 Matrices analysed:

 Food: Fruits; vegetables; grains as soya, rice, wheat, corn; wine;   juice; coffee; cocoa; processed food and so on.
 Environmental: river and drinking water; soil; biobeds and so on.

 Description of validated method used:

 1) QuEChERS (multiresidue method for LC and GC pesticide analysis)
 2) Dutch mini LUKE (multiresidue method for LC and GC pesticide           analysis)
 3) Modified QuEChERS (multiclass method for mycotoxin analysis)
 4) Single method to Patulin analysis
 5) Single residue method to dithiocarbamate analysis
 6) Single residue method to diquat and paraquat analysis

 

Pesticide Residue Laboratory- LabTox
 

 Contact person:

 Danusa Leal Telles

 Email address: 

 This email address is being protected from spambots. You need JavaScript enabled to view it.This email address is being protected from spambots. You need JavaScript enabled to view it. 

 Type of contaminants analysed:

 Pesticides, wine components, cachaça ( Brazilian Liqueur )
 Matrices analysed:  
 Fruits, Vegs, Cereal, Eater, Beverages
 Role of the laboratory:

 
 Pesticide Residue analysis

 National laboratory reference:
 Yes. We are reference Laboratory for the Ministery of
 Agriculture. We develop methodology as well as analyse samples
 from the national monitoring program.

A los Laboratorios Miembro de la RILAA

Nos complace informar que el Laboratorio Nacional Agropecuario del Ministerio de Agricultura, Pecuaria y Abastecimiento (LANAGRO-MG/MAPA) del Brasil va a organizar un ensayo de aptitud para dioxinas y furanos de relevancia toxicológica en matriz de pescado, durante el primer semestre de 2014.

Las muestras, su transporte e informe de resultados serán gratuitos, en tanto que eventuales trámites, impuestos y costos aduaneros en el país de destino deberán ser cubiertos por el Laboratorio participante.

En la dirección: http://www.eSurveysPro.com/Survey.aspx?id=c18f5db6-2c66-41ef-ac9c-559a81ac384c usted puede encontrar información detallada sobre las características del ensayo de aptitud y completar el formulario de inscripción y consultas al organizador.

Debido a que hay pocos laboratorios miembros de la RILAA que realizan estas determinaciones analíticas, podrán ser admitidos en el ensayo de aptitud "laboratorios no miembros" de otros sectores (inclusive privados). Por ello le pedimos que nos ayude a difundir este ejercicio interlaboratorio (por ejemplo, informándonos la dirección de email o reenviando este correo a quien corresponda).

Muchas gracias.

Atentamente,

Jorge E. Torroba
Secretaría ex officio de la RILAA-OPS/OMS

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